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Cerilliant Adds State-of-the-Art 400 MHz NMR System

June, 2009 – Cerilliant has upgraded its NMR system adding to the analytical capabilities of its quality control laboratory. The JEOL ECS-400 NMR has been fully qualified and represents a substantial upgrade over Cerilliant’s previous 400 MHz NMR system. The new NMR includes a shielded magnet and is equipped with gradient shimming and automatic probe tuning and matching functionality. Its analytical capabilities include the analysis of numerous paramagnetic nuclei such as 1H, 13C, 15N, 31P, and 19F. The NMR system contains software for automatic sample measurement as well as variable temperature applications for sample analysis at high or low temperatures. It also offers advanced capabilities for 2D NMR gradient experiments including COSY, NOESY, TOCSY, HMBC, and HMQC.

Most of the neat reference materials used in Cerilliant Certified Solution Standards and Certified Spiking Solutions®, including parent drugs, drugs-of-abuse, stable labeled reference materials, drug metabolites, glucuronides, and degradants are synthesized in Cerilliant’s in-house synthesis lab by our team of advanced-degreed scientists. Cerilliant also provides custom synthesis and custom analytical services to a variety of clients including pharmaceutical companies, medical device manufacturers, and researchers. The upgrade of our NMR system allows us to ensure identity of complex and obscure compounds and to monitor in-process production without delays.

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