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Improved GCMS Derivatization Techniques for Analysis of New Designer Drugs: Methylone, Ethylone, Butylone, Mephedrone, and Methedrone

Authors: Ryan Carrell, Isil Dilek, Ning Chang, Uma Sreenivasan, Yunming Ying, Greg Kirkovits
Presented at Society of Forensic Toxicologists (SOFT) / The International Association of Forensic Toxicologists (TIAFT), San Francisco, CA, September 2011

Abstract
As new ‘legal high’ drugs such as methylone, ethylone, mephedrone, butylone and other methcathinone analogs increase in popularity in the international market, toxicologists require certified native and labeled reference materials to accurately identify and quantify the new compounds. There have been problems with use of deuterated internal standards of these drugs due to loss of label in the GCMS fragmentation of the derivatized compound with PFPA and BSTFA.

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